Benzenesulfonyl chloride → HCID 178527456, compound

Participants

Reaction Steps

Prepared from N2-(2-phenoxy-ethyl)-4H-benzo[d][1,3]oxazine-2,6-diamine (Example 108, step B) (155 mg, 0.50 mmol, HPLC 0.691 min) and benzenesulfonyl chloride (70 ul, 0.55 mmol) according to the procedure described for Example 27. Obtained the title compound as an off-white foam (158 mg, 75%, HPLC 1.452 min), MS (ISP) m/e=424.1 [(M+H)+].

Provenance & Evidence