HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → HCID 178488357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | HCID 178488337 | HCID 178488337 | — |
| Product | HCID 178488357 | HCID 178488357 | 55.1% |
Reaction Steps
Prepared from rac-N2-(4-methoxy-2,3-dihydro-benzofuran-3-yl)-4H-benzo[d][1,3]oxazine-2,6-diamine (Example 6) (150 mg, 0.482 mmol) and benzenesulfonyl chloride (94 mg, 0.53 mmol) according to the procedure described for Example 27. Obtained the title compound as a white solid (120 mg, 55%), MS (ISP) m/e=452.3 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163740B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-6015f5468dde40d5bcd3f6ccecb55ded |
| Source note | uspto-grants-2012_04 |