Chloroacetyl chloride → HCID 178520799, compound

Participants

Reaction Steps

Prepared from N2-(2-phenoxy-ethyl)-4H-benzo[d][1,3]oxazine-2,6-diamine (Example 87) (591 mg, 2.0 mmol) and chloroacetyl chloride (167 ul, 2.1 mmol) according to the procedure described for Example 3 step A. Obtained the title compound as an off-white solid (585 mg, 81%), MS (ISP) m/e=360.1 [(M+H)+] and 362 [(M+2+H)+].

Provenance & Evidence