HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → N6-Benzyl-N2-(3-cyclopropyl-phenyl)-4H-benzo[d][1,3]oxazine-2,6-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | N2-(3-cyclopropyl-phenyl)-4H-benzo[d][1,3]oxazine-2,6-diamine | HCID 59231769 | — |
| Product | N6-Benzyl-N2-(3-cyclopropyl-phenyl)-4H-benzo[d][1,3]oxazine-2,6-diamine | HCID 59231904 | 67% |
Reaction Steps
Prepared from N2-(3-cyclopropyl-phenyl)-4H-benzo[d][1,3]oxazine-2,6-diamine (200 mg, 0.72 mmol) and benzaldehyde (68 mg, 0.66 mmol) according to the procedure described for example 88. Obtained the title compound as a white foam (134 mg, 67%), MS (ISP) m/e=370.1 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163740B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-ab308820c9024557b2bd90ab4acb85a7 |
| Source note | uspto-grants-2012_04 |