HRID1695687

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID91697

2,2-Dimethyl-2,3-dihydro-1-benzofuran-7-amine

C10H13NO

结构：CC(C)(C)[Si](C)(C)OCc1cc([N+](=O)[O-])ccc1N=C=S

HCID46855450

未命名化合物

PRODUCTS

生成物

结构：CC1(C)Cc2cccc(NC3=Nc4ccc([N+](=O)[O-])cc4CO3)c2O1

HCID67277608

未命名化合物

收率 67%

PROCEDURE

实验过程

Prepared from tert-butyl-(2-isothiocyanato-5-nitro-benzyloxy)-dimethyl-silane (Example C1) (3.75 g, 11 mmol) and 7-amino-2,3-dihydro-2,2-dimethylbenzofuran (CAS 68298-46-4) (1.86 g, 11 mmol) according to the procedure described for Example 1. Obtained the title compound as a yellow solid (2.5 g, 65%), MS (ISP) m/e=340.3 [(M+H)+].