1-Pyrrolidinepropanol → HCID 45268290, compound

HRID 1696686Notes

Reaction equation

[CH3:1][C:2]1[S:7][C:6]2[CH:8]=[CH:9][CH:10]=[CH:11][C:5]=2[O:4][C:3]=1[C:12]1[CH:17]=[CH:16][C:15]([OH:18])=[CH:14][CH:13]=1.O[CH2:20][CH2:21][CH2:22][N:23]1[CH2:27][CH2:26][CH2:25][CH2:24]1>>[CH3:1][C:2]1[S:7][C:6]2[CH:8]=[CH:9][CH:10]=[CH:11][C:5]=2[O:4][C:3]=1[C:12]1[CH:13]=[CH:14][C:15]([O:18][CH2:20][CH2:21][CH2:22][N:23]2[CH2:27][CH2:26][CH2:25][CH2:24]2)=[CH:16][CH:17]=1

Participants

Reactant 2

HCID 2093421-Pyrrolidinepropanol

HCID 59396727HCID 59396727, compound

Product 1

HCID 45268290HCID 45268290, compound

Procedure

The entitled compound was obtained according to the method of Example 3 but using 4-(3-methyl-1,4-benzoxathiin-2-yl)phenol synthesized in Reference Example 1-2 and 1-(3-hydroxypropyl)pyrrolidine as the starting material.

Workup

customThe entitled compound was obtained

Sources & evidence

ORD record: ord-4c55af937384479ba1937434a754f67e
Source dataset: uspto-grants-2012_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08163770B2

Reaction notes

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