1-Pyrrolidinepropanol → HCID 59396750, compound
Reaction equation
[CH2:1]([C:3]1[S:8][C:7]2[CH:9]=[CH:10][CH:11]=[CH:12][C:6]=2[O:5][C:4]=1[C:13]1[CH:18]=[CH:17][C:16]([OH:19])=[CH:15][CH:14]=1)[CH3:2].O[CH2:21][CH2:22][CH2:23][N:24]1[CH2:28][CH2:27][CH2:26][CH2:25]1>>[CH2:1]([C:3]1[S:8][C:7]2[CH:9]=[CH:10][CH:11]=[CH:12][C:6]=2[O:5][C:4]=1[C:13]1[CH:14]=[CH:15][C:16]([O:19][CH2:21][CH2:22][CH2:23][N:24]2[CH2:28][CH2:27][CH2:26][CH2:25]2)=[CH:17][CH:18]=1)[CH3:2]Participants
3
Procedure
The entitled compound was obtained according to the method of Example 3 but using 4-(3-ethyl-1,4-benzoxathiin-2-yl)phenol synthesized in Reference Example 1-3 and 1-(3-hydroxypropyl)pyrrolidine as the starting material.
Workup
- customThe entitled compound was obtained
Sources & evidence
- ORD record
- ord-15d411a41fa24e63895aff9aef023125
- Source dataset
- uspto-grants-2012_04
- Patent number
- US08163770B2
Reaction notes
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