1-Pyrrolidinepropanol → HCID 59396764, compound

HRID 1696688Notes

Reaction equation

[O:1]1[C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=2[S:4][CH2:3][CH:2]1[C:11]1[CH:16]=[CH:15][C:14]([OH:17])=[CH:13][CH:12]=1.O[CH2:19][CH2:20][CH2:21][N:22]1[CH2:26][CH2:25][CH2:24][CH2:23]1>>[N:22]1([CH2:21][CH2:20][CH2:19][O:17][C:14]2[CH:15]=[CH:16][C:11]([CH:2]3[CH2:3][S:4][C:5]4[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=4[O:1]3)=[CH:12][CH:13]=2)[CH2:26][CH2:25][CH2:24][CH2:23]1

Participants

Reactant 2

HCID 2093421-Pyrrolidinepropanol

HCID 59396720HCID 59396720, compound

Product 1

HCID 59396764HCID 59396764, compound

Procedure

The entitled compound was obtained according to the method of Example 3 but using 4-(2,3-dihydro-1,4-benzoxathiin-2-yl)phenol synthesized in Reference Example 2-4 and 1-(3-hydroxypropyl)pyrrolidine as the starting material.

Workup

customThe entitled compound was obtained

Sources & evidence

ORD record: ord-66045369f24b4ee6b653452f35a21f06
Source dataset: uspto-grants-2012_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08163770B2

Reaction notes

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