Carbon tetrabromide → HCID 67274221, compound

Participants

Reaction Steps

To a solution of 0.10 g (6-amino-4-methylsulfanyl-pyridin-2-yl)-methanol in 6 ml dichloromethane was added 0.292 g tetrabromomethane and 0.231 g triphenylphosphin and the mixture was stirred at room temperature for 1 h. The reaction mixture was purified by chromatography on silica gel with heptan:ethyl acetate=1:1 to yield 0.075 g of the title compound as white crystals MS (ISP): 232.9; 234.9 [M+H]+.

Provenance & Evidence