Hydrochloric Acid → HCID 10038987, compound

Participants

Reaction Conditions

Reaction Steps

A solution of Example 73D (120 mg) in ethanol (5 mL), and 6M HCl (5 mL) was heated in a sealed tube at 130° C. for 18 hours then cooled, concentrated to remove the ethanol, diluted with diethyl ether, cooled to 0° C., and filtered; and the filtrant was washed with ether, dried, and purified by reverse phase HPLC. NMR (300 MHz, DMSO-d6) δ 8.54 (s), 8.32 (m), 6.83 (m), 4.12 (m), 3.98 (m), 3.83 (m), 2.55 (m), 2.27 (m).

Provenance & Evidence