HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → ethyl 2-((N-methylsulfamoyl)amino)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | ethyl 2-((N-(butyloxycarbonyl)-N-methylsulfamoyl)amino)acetate | HCID 18449912 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | ethyl 2-((N-methylsulfamoyl)amino)acetate | HCID 18449915 | — |
Reaction Steps
To a solution of HCl in methanol (2 M) is added ethyl 2-((N-(butyloxycarbonyl)-N-methylsulfamoyl)amino)acetate from the previous step (5.0 mmol) in portions at RT and the mixture is stirred for 3 h. After the solvent is removed in vacuo, the residue is washed with diethyl ether to afford ethyl 2-((N-methylsulfamoyl)amino)acetate
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07737283B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-1dd420bf146b487ca19d0be0ff79813a |
| Source note | uspto-grants-2010_06 |