HRID1697748

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID78740

1-(2,2,2-Trifluoroethyl)hydrazine

C2H5F3N2

结构：COC(=O)[C@@H]1C[C@@H](S(=O)(=O)CC2CC2)CN1C(=S)CC(C)=O

HCID86646864

未命名化合物

PRODUCTS

生成物

结构：COC(=O)[C@@H]1C[C@@H](S(=O)(=O)CC2CC2)CN1c1cc(C)nn1CC(F)(F)F

HCID67278701

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described in example 192 h, (2S,4R)-4-cyclopropylmethanesulfonyl-1-(3-oxo-thiobutyryl)-pyrrolidine-2-carboxylic acid methyl ester (example 445c) was reacted with 2,2,2-trifluoroethylhydrazine (CAS Reg. No. 5042-30-8) to give the title compound as brown solid. MS (ESI): m/z=409.9 [M+H]+.