HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylhydrazine hydrochloride → HCID 67278249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylhydrazine hydrochloride | HCID 207836 | — |
| Reactant | (2S,4R)-methyl 4-(2-chlorophenylsulfonyl)-1-(3-oxobutanethioyl)pyrrolidine-2-carboxylate | HCID 86646820 | — |
| Product | HCID 67278249 | HCID 67278249 | — |
Reaction Steps
In analogy to the procedure described in example 192 h, (2S,4R)-methyl 4-(2-chlorophenylsulfonyl)-1-(3-oxobutanethioyl)pyrrolidine-2-carboxylate (example 253c) was reacted with cyclohexylhydrazine hydrochloride (CAS Reg. No. 24214-73-1) to give the title compound as orange oil. MS (ESI): m/z=466.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163793B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-eff8329b228d460da2a6e53843de2d03 |
| Source note | uspto-grants-2012_04 |