HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 59239407, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | Propyl isocyanate | HCID 61033 | — |
| Reactant | (3S)-3-methylmorpholine | HCID 12012220 | — |
| Reactant | HCID 59239109 | HCID 59239109 | — |
| Reactant | HCID 67176961 | HCID 67176961 | — |
| Product | HCID 59239407 | HCID 59239407 | — |
Reaction Steps
The title compound was prepared by the procedures described in Example 1, steps 1-5 of Example 259, and steps 1 and 2 of Example 27, by substituting morpholine with (S)-3-methylmorpholine in Example 1, (S)-3-methyl-4-(2-(4-nitrophenyl)-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidin-4-yl)morpholine with (S)-3-methyl-4-(2-(4-nitrophenyl)-6,7-dihydro-5H-pyrrolo[3,4-d]pyrimidin-4-yl)morpholine in step 1 of Example 259, and propyl isocyanate with ethyl isocyanate in step 2 of Example 27, and: LC-MS: m/z=+463 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163763B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-ac23d6ea9f014e9982a9dd953ff8392d |
| Source note | uspto-grants-2012_04 |