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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1698316Generated: November 2, 2026

Benzyl isocyanate → HCID 57870321, compound

https://huagongshe.com/reaction/1698316

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl isocyanateHCID 76639—
ReactantHCID 131729670HCID 131729670—
SolventAcetonitrileHCID 6342—
ProductHCID 57870321HCID 57870321—

Reaction Steps

The title compound is prepared analogously as described in Example 98 using (3R*,5S*)-3-amino-5-{cyclopropyl-[3-(3-methoxy-propoxy)-4-methyl-benzyl]-carbamoyl}-piperidine-1-carboxylic acid 9H-fluoren-9-ylmethyl ester, hydrochloride (Example 98A.) and benzylisocyanate. MS: 509.6 [M+H]+; tR (HPLC, Nucleosil C18; 5-100% CH3CN+0.1% TFA/H2O+0.1% TFA for 8 min, flow 1.5 ml/min): 5.22 min.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08163773B2
Source datasetuspto-grants-2012_04
ORD IDord-a11a8e56fe554714be58f700fe64bc46
Source noteuspto-grants-2012_04