HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Triisopropylsilyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Triisopropylmethoxysilane | HCID 589230 | — |
| Reactant | 1-Triisopropylsilyloxybutane | HCID 604346 | — |
| Product | Triisopropylsilyl chloride | HCID 139400 | 99% |
Reaction Steps
The procedure of Example 13 was repeated except that triisopropylmethoxysilane was replaced by 83.3 g (0.2 moles) of triisopropyl-n-butoxysilane. The latter was reacted with 35% hydrochloric acid. There was obtained 38 g of triisopropylchlorosilane (yield; 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163950B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-bad0dc197cda49cb94763d2f6877f736 |
| Source note | uspto-grants-2012_04 |