HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Benzodioxole-5-ethanamine → HCID 51301950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Benzodioxole-5-ethanamine | HCID 73874 | — |
| Reactant | 5-Isocyanato-1,3-dioxaindane | HCID 5223213 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 51301950 | HCID 51301950 | — |
Reaction Steps
A solution of 3,4-methylenedioxyphenylethylamine (0.25 g, 1.5 mmol) and 3,4-methylenedioxy-phenyl isocyanate (0.25 g, 1.5 mmol) in benzene (25 ml) was refluxed for 1 hour. The precipitate formed was filtered, washed with benzene then dried to give pure DC-0078B (0.43 g, 85%) as a pale brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163957B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-4bc788fbef294184bc11b702f6a40096 |
| Source note | uspto-grants-2012_04 |