Triethylamine → HCID 67275863, compound

Participants

Reaction Steps

To a solution of the amine obtained in step e in dichloromethane (3 mL) was added 2,4-dichlorobenzoyl chloride (210 μL, 1.5 mmol) and triethylamine (500 μL, 3.6 mmol). The reaction mixture was stirred at room temperature for 6 h. Following aqueous work-up, the residue was purified by chromatography on silica eluting with 40 to 50% ethyl acetate in hexanes to give the title compound. m/z (ES+) 427 (M+H), 425 (M+H).

Provenance & Evidence