HCID 67271832, compound → HCID 67272913, compound
Reaction equation
[CH3:1][CH2:2][CH:3]([C:7]1[C:12]2[N:13]([CH3:17])[C:14](=O)[NH:15][C:11]=2[CH:10]=[CH:9][N:8]=1)[CH2:4][CH2:5][CH3:6].[Cl:18]C1N(C)C2C(C(CCC)CCC)=CC=CC=2N=1>>[Cl:18][C:14]1[N:13]([CH3:17])[C:12]2[C:7]([CH:3]([CH2:4][CH2:5][CH3:6])[CH2:2][CH3:1])=[N:8][CH:9]=[CH:10][C:11]=2[N:15]=1Participants
3
Procedure
Prepared from 4-(hexan-3-yl)-3-methyl-1H-imidazo[4,5-c]pyridin-2(3H)-one according to the method described previously for 2-chloro-1-methyl-7-(1-propylbutyl)-1H-benzimidazole in 68% isolated yield.
Workup
- customisolated
- customyield
Sources & evidence
- ORD record
- ord-d5844c08f95e4c80b5ff2166a354b9d0
- Source dataset
- uspto-grants-2012_04
- Patent number
- US08163935B2
Reaction notes
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