HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 18551166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 17935641 | HCID 17935641 | — |
| Catalyst | Zinc cyanide (Zn(CN)2) | HCID 11186 | — |
| Product | HCID 18551166 | HCID 18551166 | — |
Reaction Steps
From 4-(4-bromo-2-methoxyphenyl)-2-hydroxy-4-methyl-2-trifluoromethyl-valeric acid ethyl ester, zinc cyanide and tetrakis-triphenylphosphine-palladium in dimethylformamide at 140° C. After saponification, the title acid is obtained as an amorphous powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06344454B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-61406f0baeb44ad3817e7fcf8584b959 |
| Source note | uspto-grants-2002_02 |