HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromocyclopentane → Ethyl 2-Cyclopentylhexan-3-onecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromocyclopentane | HCID 8728 | — |
| Reactant | Ethyl 4-oxoheptanoate | HCID 12271529 | — |
| Product | Ethyl 2-Cyclopentylhexan-3-onecarboxylate | HCID 18322313 | — |
Reaction Steps
The preparation was carried out analogously to Example I from 4.04 g (25.0 mmol) of ethyl hexan-3-onecarboxylate and 2.95 ml (4.10 g, 27.3 mmol) of bromocyclopentane. Purification was carried out chromatographically (silica gel, petroleum ether: ethyl acetate 20:1). MS (EI): 226 [M]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06344471B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-e9822307f48d44ac8c9686a642d0afb8 |
| Source note | uspto-grants-2002_02 |