HCID 86757769, compound → HCID 86757771, compound

HRID 1699126Notes

Reaction equation

HRID 1699126 reaction equation
[CH3:1][NH:2][C@H:3]([C:8]([OH:10])=[O:9])[CH2:4][CH:5]([CH3:7])[CH3:6].NC(CC=C)CC([O-])=O.CN(C(OC(C)(C)C)=O)[C@H](C(O)=O)CC(C)C.[NH2:37][CH:38]([C:43]1[CH:48]=[CH:47][C:46]2[O:49][CH2:50][O:51][C:45]=2[CH:44]=1)[CH2:39][C:40]([O-:42])=[O:41]>>[CH3:1][NH:2][C@H:3]([C:8]([OH:10])=[O:9])[CH2:4][CH:5]([CH3:7])[CH3:6].[NH2:37][CH:38]([C:43]1[CH:48]=[CH:47][C:46]2[O:49][CH2:50][O:51][C:45]=2[CH:44]=1)[CH2:39][C:40]([O-:42])=[O:41]

Participants

3

Reactant 2

HCID 86757769HCID 86757769, compoundHCID 86757772HCID 86757772, compound

Product 1

HCID 86757771HCID 86757771, compound

Procedure

This was prepared according to the method described below (example 3b) for the preparation of methyl leucine-3-amino-5-hexenoate except methyl N-(t-butoxycarbonyl)leucine-3-amino-3-(3,4-methylenedioxyphenyl)propionate was used in place of methyl N-(t-butoxycarbonyl)leucine-3-amino-5-hexenoate.

Workup

  1. customThis was prepared

Sources & evidence

ORD record
ord-fb8c454c203247719c54f8c83ad94592
Source dataset
uspto-grants-2002_02
Patent number
US06344570B1

Reaction notes

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