HCID 15550600, compound → HCID 15550601, compound

Participants

Reaction Steps

A solution of 0.14 g (0.26 mmole) of the product of step b) in 7 ml of TMS-polyphosphate was heated to 50° C. for 4 hours. The mixture was diluted to 20 ml with CH2Cl2 and washed with water and brine. The organic phase was and evaporated and the residue purified by chromatography on silica (CH2Cl2:MeOH 98:2), to give 0.11 g (82%) of the sub-title compound.

Provenance & Evidence