HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 86757782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3-Methylbenzothiazole-2(3H)-thione | HCID 75264 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86757782 | HCID 86757782 | 90% |
Reaction Steps
2.0 g (11 mmol) of 3-methylbenzothiazole-2-thione and 3.5 mL (55 mmol) of iodomethane were refluxed in 50 mL of absolute ethanol for 4 hours. Diethyl ether was added to the cooled mixture to precipitate the product. Recrystallization from ethanol:diethyl ether gave 3.2 g (90%) of pure 2-methylmercapto-3-methylbenzothiazole iodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06348317B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-5d9e8b5116424132adb820628890fb73 |
| Source note | uspto-grants-2002_02 |