Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-(3-fluoro-4-methoxyphenyl)-5-(4-methoxyphenyl)-2H-pyridazin-3-one → 2-(4-chlorocinnamyl)-6-(3-fluoro-4-methoxyphenyl)-5-(4-methoxyphenyl)-2H-pyridazin-3-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-(3-fluoro-4-methoxyphenyl)-5-(4-methoxyphenyl)-2H-pyridazin-3-one | HCID 18369367 | — |
| 반응물 | p-Chlorocinnamyl chloride | HCID 53728250 | — |
| 생성물 | 2-(4-chlorocinnamyl)-6-(3-fluoro-4-methoxyphenyl)-5-(4-methoxyphenyl)-2H-pyridazin-3-one | HCID 54242121 | 72.5% |
반응 단계
Using 6-(3-fluoro-4-methoxyphenyl)-5-(4-methoxyphenyl)-2H-pyridazin-3-one and 4-chlorocinnamyl chloride as starting materials, the procedures of Example 12 were repeated likewise, whereby the title compound was obtained in a yield of 72.5%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06348468B1 |
| 출처 데이터셋 | uspto-grants-2002_02 |
| ORD ID | ord-10f0fb7a10bf48da89d6b70ffb656aca |
| 출처 메모 | uspto-grants-2002_02 |