HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 5-methylsalicylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 5-Methylsalicylic acid | HCID 6973 | — |
| Product | Ethyl 5-methylsalicylate | HCID 118629 | — |
Reaction Steps
To a solution of 5-methyl salicylic acid (9.90 g) in ethanol (100 ml) was added concentrated sulfuric acid (1.0 g) and the mixture was refluxed under heating for 21 hr. The reaction mixture was concentrated to give an oil mainly containing the objective compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06348474B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-62f94d1214e64f07b3e386e00826d3eb |
| Source note | uspto-grants-2002_02 |