1-Phenethylamine → HCID 18317240, compound

Participants

Reaction Conditions

Reaction Steps

Under Ar, a mixture of 28 (0.62 g, 1.0 mmol) and (S) (−)-α-methylbenzylamine (1.5 mL, 11.6 mmol) was heated at 120 ° C. for 3 h. The reaction was chromatographed on a Still column (40 mm) and the product eluted with 80% EtOAc-hexanes to yield 0.6 g of 29.

Provenance & Evidence