HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylphenylhydrazine monohydrochloride → HCID 178426640, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylphenylhydrazine monohydrochloride | HCID 12504 | — |
| Reactant | HCID 21906981 | HCID 21906981 | — |
| Product | HCID 178426640 | HCID 178426640 | 41% |
Reaction Steps
1H NMR (DMSO-d6): δ 2.17 (s, 3H), 2.30 (s, 3H), 6.45 (s, 1H), 8.29 (s, 1H), 10.65 (s, 1H); ESI-MS m/z 190 (M−H)−. The isatin was combined with 4-methylphenylhydrazine hydrochloride according to Procedure H to provide the title compound in 41% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06350747B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-ebf37a534a19434ab62139773d817dc0 |
| Source note | uspto-grants-2002_02 |