HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Triethylsilyl)but-3-yn-1-yl 4-methylbenzene-1-sulfonate → HCID 12030139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Triethylsilyl)but-3-yn-1-yl 4-methylbenzene-1-sulfonate | HCID 12030138 | — |
| Reactant | HCID 86762179 | HCID 86762179 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12030139 | HCID 12030139 | — |
Reaction Steps
108 g of (4-triethylsilanylbut-3-yn-1-ol) tosylate in 50 ml of dimethylformamide are added to a suspension of 72.3 g of potassium phthalimidate in 450 ml of dimethylformamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06350757B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-f56e8cefff8f44498039b01788497239 |
| Source note | uspto-grants-2002_02 |