HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Ethylsulfonyl)ethene → HCID 53756263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Ethylsulfonyl)ethene | HCID 74680 | — |
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-methylsulfinyl-1H-pyrazole-3-carboxaldehyde oxime | HCID 136352416 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53756263 | HCID 53756263 | — |
Reaction Steps
In a manner similar to that employed in Example 12 an ethanol solution of 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-methylsulfinyl-1H-pyrazole-3-carboxaldehyde oxime was reacted with sodium ethoxide and ethyl vinyl sulfone to give 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-methylsulfinyl-1H-pyrazole-3-carboxaldehyde O-[2-(ethylsulfonyl)ethyl]oxime, m.p. 144-148° C. Compound 27.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06350771B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-5ac03598c8c84f05a663e3d59b85d528 |
| Source note | uspto-grants-2002_02 |