Thionyl Chloride → 2-Methyl-4,5-di(methylsulfonyl)benzoyl chloride

HRID 1700848Notes

Reaction equation

[CH3:1][C:2]1[CH:10]=[C:9]([S:11]([CH3:14])(=[O:13])=[O:12])[C:8]([S:15]([CH3:18])(=[O:17])=[O:16])=[CH:7][C:3]=1[C:4](O)=[O:5].S(Cl)([Cl:21])=O>>[CH3:1][C:2]1[CH:10]=[C:9]([S:11]([CH3:14])(=[O:13])=[O:12])[C:8]([S:15]([CH3:18])(=[O:17])=[O:16])=[CH:7][C:3]=1[C:4]([Cl:21])=[O:5]

Participants

Reactant 2

HCID 24386Thionyl Chloride

HCID 11266313HCID 11266313, compound

Product 1

HCID 110882142-Methyl-4,5-di(methylsulfonyl)benzoyl chloride

Procedure

in stage d) 2-methyl-4,5-di(methylsulfonyl)benzoic acid is reacted with thionyl chloride to give 2-methyl-4,5-di(methylsulfonyl)benzoyl chloride, and

Sources & evidence

ORD record: ord-ae07b7f8dd9c40fea2d656480db26ba8
Source dataset: uspto-grants-2002_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06350904B1

Reaction notes

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