HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 15453515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 1-Bromo-2-Chloroethane | HCID 7849 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4'-Fluoro-2'-hydroxyacetophenone | HCID 2737326 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 15453515 | HCID 15453515 | — |
Reaction Steps
40.5 ml of 1-bromo-2-chloroethane (490 mmol) are added to a solution of 25 g of 1-[2-hydroxy-4-fluorophenyl]ethanone (162 mmol) in 2-butanone (400 ml), followed by 45 g of potassium carbonate (320 mmol) and 1.26 g of potassium iodide (7.59 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06350913B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-22f51f15a6e24b0e8a1b603f1c08fb67 |
| Source note | uspto-grants-2002_02 |