HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodohexane → N-Hexyl-N-[2-[4-(3,3-dimethoxy-4,4,4-trifluorobut-1-yl)phenoxy]ethyl]dodecylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodohexane | HCID 12527 | — |
| Reactant | N-[2-[4-(3,3-Dimethoxy-4,4,4-trifluorobut-1-yl)phenoxy]ethyl]dodecylamine | HCID 18319017 | — |
| Reactant | N-Propyl-N-[2-[4-(4,4,4-trifluoro-3,3-dimethoxybut-1-yl)phenoxy]ethyl]dodecylamine | HCID 18319117 | — |
| Product | N-Hexyl-N-[2-[4-(3,3-dimethoxy-4,4,4-trifluorobut-1-yl)phenoxy]ethyl]dodecylamine | HCID 18319019 | 67% |
Reaction Steps
N-[2-[4-(3,3-Dimethoxy-4,4,4-trifluorobut-1-yl)phenoxy]ethyl]dodecylamine (500 mg, 1.05 mmol) and 1-iodohexane (0.186 ml, 1.26 mmol) were reacted as described in the preparation of N-propyl-N-[2-[4-(3,3-dimethoxy-4,4,4-trifluorobut-1-yl)phenoxy]ethyl]dodecylamine and afforded the title compound (390 mg, g, 67%) as a liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06350892B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-ab3711a51e2040b698b510f1c2c8e1ce |
| Source note | uspto-grants-2002_02 |