Sodium Iodide → HCID 18319096, compound

Participants

Reaction Steps

A solution of methyl 1-chloro-4,4-di-(4-chlorophenyl)butane (1.77 g, 5.64 mmol) in 2-butanone (20 ml) was treated with sodium iodide (1.5 g) and heated under reflux for 18 h. The solid formed was filtered, the filtrate was evaporated and purified on silica gel (elution hexane-toluene 96:5) to give 2.13 g (93%) of the title material as a clear oil.

Provenance & Evidence