Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 53996724 | HCID 53996724 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22949386 | HCID 22949386 | — |
Reaction Steps
5-(1-Methylamino-2-phenylethyl)-[1,2,4]oxadiazole-3-carboxylic acid ethylester (3.3 g, 9.0 mmol) was dissolved in ethanol (30 ml). Benzylamine (3 ml) was added and the reaction mixture was stirred for 18 h at 20° C. The reaction mixture was concentrated in vacuo and the residue was crystallised from ethanol to give 2.07 g of (R) 5-(1-methylamino-2-phenylethyl)-[1,2,4]oxadiazole-3-carboxylic acid benzylamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06350767B1 |
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| Source dataset | uspto-grants-2002_02 |
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| ORD ID | ord-0055007e2129487994e573f70757bbd0 |
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| Source note | uspto-grants-2002_02 |
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