HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20348064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 15872348 | HCID 15872348 | — |
| Product | HCID 20348064 | HCID 20348064 | — |
Reaction Steps
Fifteen parts of thionyl chloride or oxalyl chloride are added to 2 parts of 2,6-diphenoxybenzoic acid. The mixture is heated under reflux for 30 minutes, and the excess chloride is distilled. The residue crystallizes to give 2,6-diphenoxybenzoyl chloride, M.P. 72°-73°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04191554 |
| Source dataset | uspto-grants-1980_03 |
| ORD ID | ord-279e29f9da6640568bbee66abab2d2a6 |
| Source note | uspto-grants-1980_03 |