HRID1701091

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC[C@]12CN3CCc4c([nH]c5ccccc45)[C@@](C(=O)OC)(c4cc5c(cc4OC)N(C)[C@H]4[C@@](O)(C(=O)OC)[C@H](OC(C)=O)[C@]6(CC)C=CCN7CC[C@]54[C@@H]76)C[C@@H](C3)[C@H]1O2.O=S(=O)(O)O

HCID259897

未命名化合物

PRODUCTS

生成物

结构：CC[C@]12CN3CCc4c([nH]c5ccccc45)[C@@](C(=O)OC)(c4cc5c(cc4OC)N(C)[C@H]4[C@@](O)(C(=O)OC)[C@H](OC(C)=O)[C@]6(CC)C=CCN7CC[C@]54[C@@H]76)C[C@H](C3)[C@H]1O2

HCID442111

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID962

Water

H2O

PROCEDURE

实验过程

About 0.25 g. of leurosine sulfate were converted to the free base by dissolving the salt in water and making the resulting solution alkaline. The free base was insoluble in the aqueous alkaline layer and was extracted with chloroform. Evaporation of the chloroform yielded leurosine free base as a residue.

WORKUP

后处理

extractionwas extracted with chloroform
customEvaporation of the chloroform

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-580e176d2e18422ea17dc317244860dc
来源数据集: uspto-grants-1980_03
DOI: 10.6084/m9.figshare.5104873.v1
专利: US04191688
来源说明: uspto-grants-1980_03

反应 SMILES

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