HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12923316, compound → 2-Methyl-3-tert.-butoxypropan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12923316 | HCID 12923316 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 2-Methyl-3-tert.-butoxypropan-1-ol | HCID 12536779 | 88% |
Reaction Steps
Reduction of rac.-tert. butyl 3-tert.butoxy-2-methylpropionate was carried out with lithium aluminum hydride using the procedure described in Example 2. The resulting rac.-3-tert. butoxy-2-methyl-1-propanol was obtained in 88% yield as a colorless liquid, b.p. 70°-72° C. (10 mm Hg.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04191842 |
| Source dataset | uspto-grants-1980_03 |
| ORD ID | ord-8ede9dc7dd02442c8cc61b630dfe8d69 |
| Source note | uspto-grants-1980_03 |