HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propenoic acid, 2-cyano-3-ethoxy-, ethyl ester → Ethyl 2-cyano-3-(5-ethyl-2-pyridylamino)acrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propenoic acid, 2-cyano-3-ethoxy-, ethyl ester | HCID 78943 | — |
| Reactant | Ethyl 2-cyano-3-(5-methyl-2-pyridylamino)acrylate | HCID 4480416 | — |
| Reactant | 5-Ethylpyridin-2-amine | HCID 9812777 | — |
| Product | Ethyl 2-cyano-3-(5-ethyl-2-pyridylamino)acrylate | HCID 70593660 | 25.4% |
Reaction Steps
The title compound (m.p. 155°-156°, 25.4% yield) was prepared from 2-amino-5-ethylpyridine and ethyl ethoxymethylenecyanoacetate in a manner similar to that described for the preparation of ethyl 2-cyano-3-(5-methyl-2-pyridylamino)acrylate in Preparation 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04192944 |
| Source dataset | uspto-grants-1980_03 |
| ORD ID | ord-cf23d662f1b84f24ba3646701314fbd6 |
| Source note | uspto-grants-1980_03 |