Acetone → HCID 13071779, compound

HRID 1701479Notes

Reaction equation

HRID 1701479 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([NH:8][C:9]([NH:11][OH:12])=[O:10])[CH:5]=[CH:6][CH:7]=1.[CH3:13][C:14]([CH3:16])=O>O>[Cl:1][C:2]1[CH:3]=[C:4]([N:8]2[C:14]([CH3:16])([CH3:13])[O:12][NH:11][C:9]2=[O:10])[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 180AcetoneHCID 2695031-(3-chlorophenyl)-3-hydroxyurea

Product 1

HCID 13071779HCID 13071779, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

18.6 g. (0.1 moles) of N-(3-chlorophenyl)-N'-hydroxy-urea are added to 130 g. of acetone. The mixture is stirred for 15 minutes at the temperature of the water bath under reflux. The reaction mixture is then evaporated to dryness and the residue is recrystallized from the mixture of acetone and water.

Workup

  1. temperatureunder reflux
  2. customThe reaction mixture is then evaporated to dryness
  3. customthe residue is recrystallized from the mixture of acetone and water

Sources & evidence

ORD record
ord-22af806fe87d4c9a8427fdd7effe9bd6
Source dataset
uspto-grants-1980_03
Patent number
US04193922

Reaction notes

Loading…