HCID 12737021, compound → HCID 12737022, compound

HRID 1701513Notes

Reaction equation

HRID 1701513 reaction equation
[C:1]1([CH:7]2[CH2:12][N:11]([C:13](=[O:15])[CH3:14])[CH2:10][C:9]3[S:16][CH:17]=[CH:18][C:8]2=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C1CCCCC1.C(OCC)(=[O:27])C>>[C:1]1([CH:7]2[CH2:12][N:11]([C:13](=[O:15])[CH3:14])[C:10](=[O:27])[C:9]3[S:16][CH:17]=[CH:18][C:8]2=3)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 12737021HCID 12737021, compoundHCID 21867204Cyclohexane ethylacetate

Product 1

HCID 12737022HCID 12737022, compoundYield 20%

Procedure

The compound is prepared according to the procedure of Example 1, from 4-phenyl-6-acetyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine, to give white crystals, M.p.=132° C. (cyclohexane-ethyl acetate), Yield: 20%.

Workup

  1. customThe compound is prepared

Sources & evidence

ORD record
ord-29f4bfb284604ad1a03a77a6dee9ab3f
Source dataset
uspto-grants-1980_03
Patent number
US04193997

Reaction notes

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