Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1701715Generated: October 31, 2026

Water → Acetic acid, ((4-(3-furanylcarbonyl)-1-naphthalenyl)oxy)-

https://huagongshe.com/reaction/1701715

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantPotassium CarbonateHCID 11430—
ReactantEthyl [(naphthalen-1-yl)oxy]acetateHCID 1482829—
SolventEthanolHCID 702—
ProductAcetic acid, ((4-(3-furanylcarbonyl)-1-naphthalenyl)oxy)-HCID 3052164—

Reaction Steps

15 g of the ester obtained according to (a) are dissolved in 300 ml ethanol; after addition of 7.6 g potassium carbonate in solution in 25 ml water, the mixture is refluxed for 17 hours and the alcohol removed under reduced pressure. The residue is purified by dissolution in water; the final product is extracted from the aqueous phase after acidification. 12 g of the acid which, after recrystallisation from dichloroethane, melts at 177° C. are obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04195093
Source datasetuspto-grants-1980_03
ORD IDord-703fd5c5c37843c7b538caf41730490b
Source noteuspto-grants-1980_03