Thionyl Chloride → HCID 20346151, compound
Reaction equation
[S:1]([C:5]1[CH:6]=[C:7]([C:10]([OH:12])=O)[O:8][CH:9]=1)([OH:4])(=[O:3])=[O:2].S(Cl)([Cl:15])=O>>[S:1]([C:5]1[CH:6]=[C:7]([C:10]([Cl:15])=[O:12])[O:8][CH:9]=1)([OH:4])(=[O:3])=[O:2]Participants
3
Procedure
4-Sulfo-2-furoic acid (0.1 mole) is stirred with 30 ml of thionyl chloride (SOCl2) for 40 minutes at 60° C. The reaction mixture is evaporated to dryness to give 4-sulfo-2-furoyl chloride.
Workup
- customThe reaction mixture is evaporated to dryness
Sources & evidence
- ORD record
- ord-b02aa1619458402c9effc95330045d17
- Source dataset
- uspto-grants-1980_03
- Patent number
- US04195023
Reaction notes
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