HuagongsheHuagongshe Chemistry Print Report · For research reference only
Penicillin G → HCID 56975303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Penicillin G | HCID 5904 | — |
| Reactant | Lithium Chloride | HCID 433294 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | tert-Butanol | HCID 6386 | — |
| Product | HCID 56975303 | HCID 56975303 | 88% |
Reaction Steps
A 6.2 mg quantity of lithium chloride was dissolved in a mixture of 2 ml of methanol and 0.5 ml of tert-butyl alcohol. To the solution was added 62.4 mg of benzyl ester of penicillin G to prepare an electrolyte. The electrolyte was subjected to electrolysis under the same conditions as in Example 1. The isolation and purification gives 50 mg of contemplated compound in 88% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04379032 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-2bb35a46482e4a6e86eb81daed9663a3 |
| Source note | uspto-grants-1983_04 |