HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-Nitrothiazole → 2-nitro-N-(5-nitro-1,3-thiazol-2-yl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-Nitrothiazole | HCID 8486 | — |
| Reactant | 2-Nitrobenzoyl chloride | HCID 11875 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2-nitro-N-(5-nitro-1,3-thiazol-2-yl)benzamide | HCID 321578 | — |
Reaction Steps
By following the procedure of the first part of Example 1, but using 2-nitrobenzoyl chloride (18.5 g), 2-amino-5-nitrothiazole (14.5 g) and pyridine (ca 80 ml), there was obtained 2-nitro-N-(5-nitro-2-thiazolyl)-benzamide, m.pt 248°-250°, after crystallization from 2-methoxyethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04379156 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-cac03bb0ec004497bb492e2ec43f2cea |
| Source note | uspto-grants-1983_04 |