Allyl bromide → HCID 13116875, compound

HRID 1701839Notes

Reaction equation

HRID 1701839 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[CH:12]([C:13]3[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][CH:14]=3)[NH:11][C:10]([SH:20])=[N:9]2)=[CH:4][CH:3]=1.[CH2:21](Br)[CH:22]=[CH2:23]>>[ClH:1].[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH:8]2[CH:12]([C:13]3[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][CH:14]=3)[NH:11][C:10]([S:20][CH2:23][CH:22]=[CH2:21])=[N:9]2)=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 7841Allyl bromideHCID 178527834HCID 178527834, compound

Product 1

HCID 13116875HCID 13116875, compound

Procedure

By the procedure described in Example 1, 2.0 g of 4,5-bis(4-chlorophenyl)-4,5-dihydro-1H-imidazole-2-thiol was converted to 1.0 g of the title compound with allyl bromide. After recrystallization from nitromethane, the colorless crystals had m.p. 208° dec. The infrared and NMR spectra of the free base were consistent with the proposed structure.

Sources & evidence

ORD record
ord-c091b43c420f4dc891d47e50ecef035b
Source dataset
uspto-grants-1983_04
Patent number
US04379159

Reaction notes

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