Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 3-Chloro-2-cyanobenzenesulfonyl chloride | HCID 18974428 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 54377672 | HCID 54377672 | — |
Reaction Steps
7.1 g of 2-cyano-3-chlorobenzenesulphonylchloride were added to a solution of 9 ml of methylamine in approx. 15 ml of water cooled at 0° C. After stirring at 0°-10° C. for 1 hour, the solid was sucked off, washed with water and dried in air. The desired product was obtained in a yield of 5,5 g; melting-point 140°-142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04379157 |
|---|
| Source dataset | uspto-grants-1983_04 |
|---|
| ORD ID | ord-d75be56b262d4a139d3024ef1503cc6c |
|---|
| Source note | uspto-grants-1983_04 |
|---|
