HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1701854Generated: November 4, 2026
Cyclopropanemethanamine → HCID 13647243, compound
https://huagongshe.com/reaction/1701854
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Cyclopropanemethanamine | HCID 75646 | — |
| Reactant | HCID 264235 | HCID 264235 | — |
| Product | HCID 13647243 | HCID 13647243 | 62.6% |
Reaction Steps
78 g of cyclopropylmethylamine (1.1 mole) and 220 g of 3-hexenedioic acid diethyl ester are introduced into a liter autoclave. The mixture is heated to 165° C. and then kept at that temperature for 8 hours. After cooling, the product is distilled under vacuum, first eliminating the alcohol, then obtaining 155 g of a compound which distils at 157°-160° C. under 3 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04379161 |
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| Source dataset | uspto-grants-1983_04 |
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| ORD ID | ord-265611e3ddf74372ad97174a7d41eb4c |
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| Source note | uspto-grants-1983_04 |
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