Ammonium benzoate → Zinc

HRID 1701985Notes

Reaction equation

HRID 1701985 reaction equation
[O-2].[Zn+2:2].[C:3]([O-])(=[O:10])C1C=CC=CC=1.[NH4+].[CH:13]1([C:19]2[CH:24]=[CH:23][C:22]([OH:25])=[CH:21][CH:20]=2)[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1.[C:26]1([OH:32])[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1.C=O>>[Zn:2].[CH:13]1([C:19]2[CH:20]=[CH:21][C:22]([OH:25])=[CH:23][CH:24]=2)[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18]1.[C:26]1([OH:32])[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1.[CH2:3]=[O:10]

Participants

5

Reactant 3

HCID 15830Ammonium benzoateHCID 3007857Zinc OxideHCID 86738833HCID 86738833, compound

Product 2

HCID 23994ZincHCID 86738833HCID 86738833, compound

Procedure

A mixture of 3.7 g of zinc oxide (JIS No. 1) and 15.0 g of ammonium benzoate was gradually added to 100 g of the above p-cyclohexylphenol/phenol/formaldehyde co-condensate kept at 170° C. with stirring, and they were reacted at 165° to 170° C. for 1.5 hours to give a pale yellow transparent zinc salt of the p-cyclohexylphenol/phenol/formaldehyde co-condensate.

Workup

  1. customkept at 170° C.
  2. customthey were reacted at 165° to 170° C. for 1.5 hours

Sources & evidence

ORD record
ord-78bc3180a08946ab8378b73c98439457
Source dataset
uspto-grants-1983_04
Patent number
US04379897

Reaction notes

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