HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 13178698, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 13178695 | HCID 13178695 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 13178698 | HCID 13178698 | — |
Reaction Steps
The bromination of 1-(2,4-dichlorophenyl)-4,4-dimethyl-1-(4-chlorophenylsulfonyl)-pentan-3-one was carried out in the same manner as that of Example 3 but using 25 g of 1-(2,4-dichlorophenyl)-1-(4-chlorophenylsulfonyl)-4,4-dimethylpentan-3-one, 8.9 g of bromine, 200 ml of acetic acid and 300 ml of chloroform, and 24.4 g of 2-bromo-1-(2,4-dichlorophenyl)-4,4-dimethyl-1-(4-chlorophenylsulfonyl)pentan-3-one was obtained. m.p. 184°-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04379921 |
| Source dataset | uspto-grants-1983_04 |
| ORD ID | ord-c76dcc22c22646c8b1a68a65a5b78549 |
| Source note | uspto-grants-1983_04 |